The solvent was removed under vacuum, and the resulting blue solid residue was washed with Et 2 O (3 × 10 mL) Complex Ni1 was obtained as a blue solid (0.24 g, 88%) Method B: to a solution of NiCl 2 (dme) (0.10 g, 0.46 mmol) and LiCl (0.019 g, 0.46 mmol) in CH 2 Cl 2 (5 mL) was added a 1, mL), and the resulting solution was stirred for 20 h at room temperature (f) J. Skupinska, pp.717-235, 1983. ,
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