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Synthesis of Quinolines Through Acceptorless Dehydrogenative Coupling Catalyzed by Rhenium PN(H)P Complexes

Abstract : A practical and sustainable synthesis of substituted quinolines was achieved through the annulation of 2-aminobenzyl alcohol with various secondary alcohols, ketones, aldehydes, or nitriles, under hydrogen-borrowing conditions. Under the catalysis of well-defined rhenium complexes bearing tridentate diphosphinoamino ligands, the reaction proceeded efficiently (31 examples were isolated with yields up to 96 %) affording a variety of quinoline derivatives.
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Duo Wei, Vincent Dorcet, Christophe Darcel, Jean-Baptiste Sortais. Synthesis of Quinolines Through Acceptorless Dehydrogenative Coupling Catalyzed by Rhenium PN(H)P Complexes. ChemSusChem, ChemPubSoc Europe/Wiley, 2019, 12 (13), pp.3078-3082. ⟨10.1002/cssc.201802636⟩. ⟨hal-02019486⟩

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