, Acta Cryst, vol.76, pp.273-275, 2020.
, N2-Zn1-N3 89.15 (16) C21-C26-H26 118.3 N1-Zn1-N3 167.43 (17) C25-C26-H26 118.3 N4-Zn1-N3, vol.88, pp.24-27
, N2-Zn1-O60 i 91.84 (16) O27-C28-H28A 109.5 N1-Zn1-O60 i 91.71 (16) O27-C28-H28B 109.5 N4-Zn1-O60 i 99.90 (17) H28A-C28-H28B 109.5 N3-Zn1-O60 i, vol.100, pp.27-28
, C1-N1-C18, vol.106
, C1-N1-Zn1 126.3 (3) H28B-C28-H28C 109.5 C18-N1-Zn1, vol.126, pp.32-63
, C6-N2-C3, vol.106, pp.32-63
, C6-N2-Zn1, vol.127, pp.36-67
, C8-N3-C11 107.5 (4) C31-C32-H32 120.2 C8-N3-Zn1 125.4 (3) C33-C32-H32 120.2 C11-N3-Zn1, vol.126, pp.34-67
, C13-N4-C16 106.8 (4) C34-C33-H33 118.8 C13-N4-Zn1, vol.127, pp.33-34
, C3-C2-C1 125.1 (5) C36-C35-H35 120.2 C3-C2-C21 117.1 (4) C34-C35-H35 120.2 C1-C2-C21 117, vol.7, pp.35-36
, C2-C3-N2 126.5 (4) C35-C36-H36 119.1 C2-C3-C4 125.4 (4) C31-C36-H36 119.1 N2-C3-C4, vol.108
, N2-C6-C7 125.6 (4) C42-C41-C46 117.4 (5) N2-C6-C5 111, vol.2, pp.42-83
, , vol.123
, C8-C7-C6, vol.124, pp.41-42
, (5) C42-C43-H43 120.4 C7-C8-C9 123.3 (5) C44-C43-H43 120.4 C10-C9-C8 105, vol.8, pp.47-91
, C10-C9-H9 127.2 O47-C44-C45, vol.116
, C8-C9-H9 127, vol.2, pp.43-44
, Acta Cryst, vol.76, pp.273-275, 2020.
, C9-C10-C11, vol.107, pp.46-91
, C9-C10-H10 126.1 C46-C45-H45 120.0 C11-C10-H10 126.1 C44-C45-H45 120.0 N3-C11-C12 126, vol.6, pp.45-46
, N3-C11-C10 108.9 (4) C45-C46-H46 118.8 C12-C11-C10 124.5 (5) C41-C46-H46 118.8 C13-C12-C11, vol.124, pp.44-47
, C13-C12-C31 118.1 (5) O47-C48-H48A 109.5 C11-C12-C31 117.8 (5) O47-C48-H48B 109.5 N4-C13-C12 126.0 (5) H48A-C48-H48B 109.5 N4-C13-C14 109.8 (4) O47-C48
, C13-C14-H14 126, vol.6, pp.53-54
, C14-C15-C16, vol.107, pp.55-54
, C14-C15-H15 126.3 C56-C55-C54 121, vol.2
, C16-C15-H15 126.3 C56-C55-H55 119.4 N4-C16-C17 126.6 (4) C54-C55-H55 119.4 N4-C16-C15, vol.109
, C17-C16-C15 124.2 (4) C55-C56-H56 119.7 C18-C17-C16 124.4 (4) C51-C56-H56 119.7 C18-C17-C51 118, vol.7, pp.52-51
, N1-C18-C17 126.4 (4) C56-C51-C17 120.5 (5) N1-C18-C19, vol.109, pp.51-52
, C17-C18-C19, vol.124, pp.51-52
, O27-C24-C25 125.7 (6) N62-C61-H61 119.9 C23-C24-C25 117.8 (5) C59-C61-H61 119.9 C26-C25-C24, vol.119
, C18-N1-C1-C2, vol.178, pp.51-68
, Acta Cryst, vol.76, pp.273-275, 2020.
, , vol.9
, C20-C1-C2-C3 178.3 (5) C2-C1-C20-C19 ?179.5 (5) N1-C1-C2-C21 ?177.4 (5) C3-C2-C21-C26 ?77, vol.8
, C21-C2-C3-N2 177, vol.7
, , vol.179
, C21-C2-C3-C4 ?0, vol.9
, C6-N2-C3-C2, vol.179
, Zn1-N2-C3-C2 8.7 (8) C22-C23-C24-O27, vol.174
, , vol.172
, C2-C3-C4-C5 179.5 (5) C23-C24-C25-C26 1.3 (10) N2-C3-C4
, C3-C4-C5-C6 0.2 (6) C2-C21-C26-C25, vol.176
, C3-N2-C6-C7 ?178.5 (5) C24-C25-C26-C21, vol.2
, Zn1-N2-C6-C7 ?7.5 (7) C23
, C3-N2-C6-C5, vol.1
, Zn1-N2-C6-C5, vol.172
, C4-C5-C6-N2 ?1.0 (6) C11-C12-C31-C32, vol.64
, C4-C5-C6-C7 178.9 (5) C13-C12-C31-C36 63.4 (7) N2-C6-C7-C8 ?1.3 (8) C11-C12-C31-C36 ?117, vol.7
, C5-C6-C7-C8 178.8 (5) C36-C31-C32-C33 ?0.2 (8) N2-C6-C7-C41 176.3 (5) C12-C31-C32-C33 177, vol.7
, , vol.3
, C11-N3-C8-C7, vol.179
, Zn1-N3-C8-C7, vol.6
, Zn1-N3-C8-C9 ?, vol.171
, C6-C7-C8-N3 1.5 (8) C34-C35-C36-C31 1.2 (9) C41-C7-C8-N3 ?176.1 (5) C32-C31-C36-C35 0.1 (8) C6-C7-C8-C9 ?179.8 (5) C12-C31-C36-C35 ?, vol.177
, C41-C7-C8-C9 2.6 (8) C33-C34-O37-C38 ?177.4 (6) N3-C8-C9-C10 ?0.6 (7) C35-C34-O37-C38, vol.2
, C8-C9-C10-C11 0.6 (7) C6-C7-C41-C42 ?96, vol.7
, C8-N3-C11-C12 ?178.4 (5) C8-C7-C41-C46 ?95, vol.9
, , vol.6
, C8-N3-C11-C10 0.1 (6) C46-C41-C42-C43 ?, vol.1
, Zn1-N3-C11-C10 172.2 (4) C7-C41-C42-C43 ?178
, C9-C10-C11-N3 ?0.5 (7) C41-C42-C43-C44, vol.2
, C9-C10-C11-C12 178.0 (5) C42-C43-C44-O47 ?179, vol.2
, N3-C11-C12-C13 ?, vol.1
, C10-C11-C12-C13, vol.179
, N3-C11-C12-C31, vol.179, p.10
, Acta Cryst, vol.76, pp.273-275, 2020.
, C16-N4-C13-C12 ?179.4 (5) C42-C41-C46-C45 ?, vol.1
, Zn1-N4-C13-C12 6.5 (8) C7-C41-C46-C45, vol.175
, Zn1-N4-C13-C14 ?175.3 (4) C45-C44-O47-C48 ?, vol.177
, C11-C12-C13-N4 1.8 (8) C53-C54-C55-C56 2.2 (9) C31-C12-C13-N4 ?179.5 (5) C57-C54-C55-C56, vol.177
, C11-C12-C13-C14 ?, vol.176
, C31-C12-C13-C14 2.6 (8) C55-C56-C51-C52 ?0, vol.8
, N4-C13-C14-C15 1.3 (7) C55-C56-C51-C17, vol.178
, C12-C13-C14-C15, vol.179
, C13-C14-C15-C16 ?0, vol.9
, C13-N4-C16-C17, vol.178
,
, C13-N4-C16-C15 0.7 (6) C56-C51-C52-C53 1.5 (8) Zn1-N4-C16-C15, vol.174
, C14-C15-C16-C17 ?, vol.177
, N4-C16-C17-C18, vol.1
, C15-C16-C17-C18 178.5 (5) C57-O58-C59-O60 ?2.9
, , vol.178
, C15-C16-C17-C51 ?1.0 (7) C59-O58-C57-C54, vol.86
, C1-N1-C18-C17, vol.178
, Zn1-N1-C18-C17 6.0 (7) C55-C54-C57-O58 76
, C1-N1-C18-C19 0.5 (6) O58-C59-O60-Zn1 ii, vol.174
, ) C61-C59-O60-Zn1 ii ?8, Zn1-N1-C18-C19 ?171, vol.7
, C16-C17-C18-N1 ?0.4 (8) O60-C59-C61-N62 ?, vol.174
, C51-C17-C18-N1 179.1 (5) O58-C59-C61-N62, vol.2
, C16-C17-C18-C19, vol.176
, Symmetry codes: (i) x?1, y, z; (ii) x+1, y, z